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Beilstein J. Org. Chem. 2010, 6, 1211–1218, doi:10.3762/bjoc.6.139
Graphical Abstract
Figure 1: Synthesized compounds 1 and 2.
Scheme 1: Syntheses of 1 and 2.
Figure 2: Change in 1H NMR of (A) 1 (400 MHz, CDCl3 containing 0.4% d6-DMSO; c = 2.80 × 10−3 M) and in the pr...
Figure 3: Change in fluorescence ratio of 1 upon addition of one equivalent of anions (c = 4.31 × 10−5 M) at ...
Figure 4: Change in emission of 1 (c = 4.31 × 10−5 M) upon gradual addition of tetrabutylammonium salts of (a...
Figure 5: Suggested modes of binding of the amino acid salts into the open cleft of 1.
Figure 6: Fluorescence titration curves for 1 (c = 4.31 × 10−5 M) at 492 nm.
Figure 7: Fluorescence decays (at λmax = 420 nm) of receptor 1 upon the addition of 1 equiv of L-N-acetylvali...
Figure 8: Change in absorbance of 1 (c = 4.31 × 10−5 M) upon gradual addition of tetrabutylammonium salts of ...
Figure 9: DFT optimized geometry of the complex of 1 with L-N-acetylvaline carboxylate salt [a = 1.93 Å, b = ...